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  • Polymer Kit 2.0: Reference materials to help standardize microplastics research

    April 16, 2024

    Collaborators

    • Brett Howard
      American Chemistry Council
      (Washington, DC, US)
    • John Norman
      American Chemistry Council
      (Washington, DC, US)
    • Jennifer M. Lynch
      National Institute of Standards and Technology & Hawaii Pacific University Center for Marine Debris Research
      (Hawaii, US)
    • Kellie Teague
      Hawaii Pacific University Center for Marine Debris Research
      (Hawaii, US)
    • Chase Thompson
      National Institute of Standards and Technology
      (Maryland, US)
    • Meredith Seeley
      National Institute of Standards and Technology
      (Maryland, US)
    • Katherine Shaw
      National Institute of Standards and Technology
      (Maryland, US)

    Timeline

    Donated materials were received in December 2022. Two LDPE powders will be ready to market in 2024.

    Additional information

    Two polyethylene microplastic materials were well-characterized to provide researchers with standardized materials for microplastic research. Analysis of materials included use of various polymer identification methods, including attenuated total reflectance-Fourier transform infrared spectroscopy (ATR FTIR), differential scanning calorimetry (DSC), uFTIR in reflectance mode, uRaman, py-GCMS, and HT-SEC.

    Professional Presentations

    N/A

    Published Papers

    N/A

  • Polymer Kit 1.0: Reference materials to help standardize microplastics research

    April 16, 2024

    Collaborators

    • Brett Howard
      American Chemistry Council
      (Washington, DC, US)
    • Jennifer M. Lynch
      National Institute of Standards and Technology & Hawaii Pacific University Center for Marine Debris Research
      (Hawaii, US)
    • Kellie Teague
      Hawaii Pacific University Center for Marine Debris Research
      (Hawaii, US)
    • Raquel Corniuk
      Hawaii Pacific University Center for Marine Debris Research
      (Hawaii, US)

    Timeline

    Funding and polymers were received in June 2020; Polymer Kit 1.0 was completed and launched onto the market in November 2020.

    Additional information

    https://www.hpu.edu/cncs/cmdr/img/polymerkit1.0_marketingbrochure.pdf

    Professional Presentations

    Polymer Kit 1.0 – To Harmonize Plastic Pollution Research, Pacific Northwest Consortium on Plastics (virtual)

    Polymer Kit 1.0 – Usefulness of Polymer Reference Materials in Marine Debris Analyses, SETAC North America (virtual)

    Usefulness of Polymer Reference Materials in Marine Debris Analyses, PacifChem (virtual)

    Published Papers

    N/A

  • Method development for the extraction of microplastics from sediment

    April 16, 2024

    Collaborators

    • Katherine Shaw
      National Institute of Standards and Technology
      (Hawaii, US)
    • Rachel Sandquist
      Hawaii Pacific University Center for Marine Debris Research
      (Hawaii, US)
    • Cameron Fairclough
      CoastalOceanVision
      (Massachusetts, US)
    • Scott Gallager
      CoastalOceanVision
      (Massachusetts, US)
    • Jennifer M. Lynch
      National Institute of Standards and Technology and Hawaii Pacific University Center for Marine Debris Research
      (Hawaii, US)

    Timeline

    Estimated publication date of study findings, March 2023.

    Additional Information

    Professional Presentations

    A Novel Method for the Extraction of Microplastics from Marine Sediment, PacifiChem (virtual)

    Effective microplastic extraction from deep sea sediment with an affordable and easily accessible density separation device, 7th International Marine Debris Conference (IMDC; Busan, Republic of Korea), September 18-23, 2022

    Published Papers

    Separation of microplastics from deep-sea sediment using an affordable, simple to use, and easily accessible density separation device, in review

  • Reliably generating microplastic particles using novel methods

    April 16, 2024

    Collaborators

    • Christie Sayes, Taiwo Ayorinde & Joaquin Lugo
      Baylor University and CS Consulting
      (Texas, US)

    Timeline

    Q3 2024

    Additional information

    Professional Presentations

    N/A

    Published Papers

    N/A

  • Development of silicon nanomembrane analysis pipelines (SNAPs) to characterize microplastics

    April 13, 2024

    Researchers / Institutional Affiliations

    Co-principal Investigators

    • Dr. Samantha Romanick
      Postdoctoral Fellow
      University of Rochester
      River Campus
      Department of Biomedical Engineering
      (US)
    • Dr. James McGrath
      Professor
      University of Rochester
      River Campus
      Department of Biomedical Engineering
      (US)

    Collaborators

    • Dr. Greg Madejski
      Nano Laboratory Engineer
      University of Rochester
      River Campus
      Department of Biomedical Engineering
      (Rochester, NY, US)
    • Dr. Alison Elder
      Professor
      University of Rochester Medical Center
      Department of Environmental Medicine
      (Rochester, NY, US)
    • Dr. Stavros Demos
      Distinguished Scientist
      University of Rochester
      Laboratory of Laster Energetics
      (Rochester, NY, US)
    • Nathan Eddingsaas
      Associate Professor of Chemistry
      Rochester Institute of Technology
      School of Chemistry and Materials Science
      (Rochester, NY, US)

    Timeline

    Project is expected to be completed by September 2024 with publication of findings to follow in late 2024 or early 2025.

    Additional information

    Microplastics are found in natural waters and in foods and drinks derived from these waters; microplastics are thus ingested and inhaled by humans and found in human tissues. Research on microplastics is challenging due to the labor-intensive protocols associated with isolating them from the environment and biological tissues, particularly at the size scales most relevant to human health (<20μm). Due to lack of well characterized commercial reference MPs, toxicity researchers often resort to commercially available polystyrene spheres, which are a poor model for the environmental microplastics that are most relevant to human health. As novel time-saving protocols, silicon nanomembrane analyses pipelines (SNAPs) are being used with reference and environmental microplastics. In these methods, raw samples are added to nanomembranes housed in filtration devices. The samples are serially processed here until ready for imaging or spectroscopic analysis. The SNAP protocols are reproducible and rigorous and will be used in future studies to characterize environmental microplastics.

    The grant title for this project is, ‘Characterization of Highly Referenced Commercial Monodispersed Microplastics Test Materials.’

    Professional Presentations

    N/A

    Published Papers

    N/A

  • Microplastics systematic review for mammalian developmental and reproductive toxicity endpoints

    April 13, 2024

    Researchers / Institutional Affiliations

    • Seneca Fitch, Daniele Wikoff & John Rogers
      ToxStrategies, LLC
      (US)
    • Steffen Schneider & Bjoern Hidding
      BASF
      (Germany)
    • Sue Marty & Robert Ellis-Hutchings
      Dow, Inc
      (US)
    • Erik Rushton
      LyondellBasell
      (The Netherlands)

    Timeline

    Completion 3Q24

    Additional Information

    Professional Presentations

    Fitch S, Rogers J, Marty S, Ellis-Hutchings R, Becker R, Wikoff D. Development of a Study Quality Tool for Use in a Systematic Review of Literature Reporting Microplastic Exposure and
    Reproductive and Developmental Toxicity
    . Society of Toxicology’s 62nd Annual Meeting, March 2023, Nashville Tennessee (US).

    Fitch S, Ellis-Hutchings R, Rogers J, Marty S, Rushton E, Schneider S, Otte J, Norman J, Wikoff D. Study quality evaluation of literature reporting plastic microparticle exposure against
    reproductive and developmental toxicity endpoint. Society of Toxicology’s 63rd Annual Meeting, March 2024, Salt Lake City, Utah (US).

    Published Papers

    (IN DRAFT) Seneca Fitch, John Rogers, Allison Franzen, Robert Ellis-Hutchings, Sue Marty, Jens Otte, Erik Rushton, Susan Borghoff, Daniele Wikoff. DRAFT. Systematic Review of Microplastics and Potential Developmental and Reproductive Toxicity. Unsubmitted.

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